HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → 3-[[Acetyl[[4-(tetradecyloxy)phenyl]methyl]amino]methyl]-1-methylpyridinium iodide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | N-(3-Pyridinylmethyl)-N-[[4-(tetradecyloxy)phenyl]methyl]acetamide | HCID 10026896 | — |
| Product | 3-[[Acetyl[[4-(tetradecyloxy)phenyl]methyl]amino]methyl]-1-methylpyridinium iodide | HCID 10008641 | — |
Reaction Steps
The title compound is prepared by the procedure of Example 28 using 0.492 g of product from Example 73 and 3.38 ml of methyl iodide. The residue is purified by crystallization to give 0.64 g of the desired product as orange crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05208247 |
| Source dataset | uspto-grants-1993_05 |
| ORD ID | ord-878345184f42497995c187a2a57b7046 |
| Source note | uspto-grants-1993_05 |