HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → 4-[[Acetyl[[4-(tetradecyloxy)phenyl]methyl]amino]methyl]-1-methylpyridinium iodide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | N-(4-Pyridinylmethyl)-N-[[4-(tetradecyloxy)phenyl]methyl]acetamide | HCID 10095404 | — |
| Product | 4-[[Acetyl[[4-(tetradecyloxy)phenyl]methyl]amino]methyl]-1-methylpyridinium iodide | HCID 10348470 | — |
Reaction Steps
The title compound is prepared by the procedure of Example 28 using 0.741 g of product from Example 77 and 5.1 ml of methyl iodide. The residue is recrystallized from methyl alcohol to give 0.933 g of the desired product as orange crystals. The spectral data indicates 2 rotomers.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05208247 |
| Source dataset | uspto-grants-1993_05 |
| ORD ID | ord-a7a67a5028fe423881be2052c166e8ef |
| Source note | uspto-grants-1993_05 |