HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Nitrophenyl tetradecyl ether → p-(n-Tetradecyloxy)phenylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Nitrophenyl tetradecyl ether | HCID 10337051 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | p-(n-Tetradecyloxy)phenylamine | HCID 191002 | 94.1% |
Reaction Steps
A solution of 30 g of product from Example 81 in 150 ml of ethyl alcohol and 20 ml of ethyl acetate is treated with 2 g of 10% palladium/carbon in a Parr Hydrogenator for 18 hours. The reaction solution is filtered and concentrated in vacuo. The residue is recrystallized from hexane to give 25.7 g of the desired product as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05208247 |
| Source dataset | uspto-grants-1993_05 |
| ORD ID | ord-4f774d62cf354237a48ef823dcaa5de5 |
| Source note | uspto-grants-1993_05 |