HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 248016Generated: October 30, 2026
Methyl iodide → 2-[[Acetyl[3,4-bis(heptyloxy)benzoyl]amino]methyl]-1-methylpyridinium iodide
https://huagongshe.com/reaction/248016
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | N-Acetyl-3,4-bis(heptyloxy)-N-(2-pyridinylmethyl)benzamide | HCID 10367999 | — |
| Product | 2-[[Acetyl[3,4-bis(heptyloxy)benzoyl]amino]methyl]-1-methylpyridinium iodide | HCID 10326597 | 95.8% |
Reaction Steps
A mixture of 1.0 g of product from Example 112 and 14.7 g of methyl iodide is heated in a sealed tube at 105° C. from 171/4 hours. The reaction is concentrated in vacuo to give 1.24 g of the desired product as yellow crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05208247 |
|---|
| Source dataset | uspto-grants-1993_05 |
|---|
| ORD ID | ord-af3ebb80beb64d97b111e0ba717ba4df |
|---|
| Source note | uspto-grants-1993_05 |
|---|
