HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 10326368, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | N-Acetyl-4-(decyloxy)-3-(1,1-dimethylethyl)-N-(2-pyridinylmethyl)benzamide | HCID 10367290 | — |
| Product | HCID 10326368 | HCID 10326368 | 91.4% |
Reaction Steps
A mixture of 1.56 g of product from Example 133 and 23.68 g of methyl iodide is heated in a sealed tube, in the dark, at 105° C. for 18 hours. The reaction is concentrated in vacuo to give 1.86 g of the desired product as light yellow crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05208247 |
| Source dataset | uspto-grants-1993_05 |
| ORD ID | ord-0967f180f2c041de802fe24dc414b189 |
| Source note | uspto-grants-1993_05 |