Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 1-Iodopropane | HCID 33643 | — |
| Reactant | HCID 19015330 | HCID 19015330 | — |
| Product | HCID 19015355 | HCID 19015355 | 99.9% |
Reaction Steps
A mixture of 0.80 g of product from Example 146 and 13.58 g of iodopropane is heated, in a sealed tube, at 100° C. for 10 hours. The reaction is concentrated in vacuo to give 1.07 g of the desired product as orange crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05208247 |
|---|
| Source dataset | uspto-grants-1993_05 |
|---|
| ORD ID | ord-91dd6c2a47764890b94a9b4035ed89f1 |
|---|
| Source note | uspto-grants-1993_05 |
|---|
