HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methylbenzenethiol → 3-Bromo-5-trifluoromethylphenyl 4-tolyl sulphide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methylbenzenethiol | HCID 7811 | — |
| Reactant | 3-Bromo-5-fluorobenzotrifluoride | HCID 2736323 | — |
| Product | 3-Bromo-5-trifluoromethylphenyl 4-tolyl sulphide | HCID 19764849 | 63% |
Reaction Steps
Using a similar procedure to that described in the 1st paragraph of Note a. above 4-toluenethiol was reacted with 1-bromo-3-fluoro-5-trifluoromethylbenzene to give 3-bromo-5-trifluoromethylphenyl 4-tolyl sulphide in 63% yield as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05208259 |
| Source dataset | uspto-grants-1993_05 |
| ORD ID | ord-bdb4bed397164cd9a7fef44ca74741dc |
| Source note | uspto-grants-1993_05 |