HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Bromonaphthalene-2-thiol → 4-[3-(6-Bromonaphth-2-ylthio)phenyl]-4-methoxytetrahydropyran
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Bromonaphthalene-2-thiol | HCID 19764817 | — |
| Reactant | 4-(3-Iodophenyl)-4-methoxytetrahydropyran | HCID 19764856 | — |
| Product | 4-[3-(6-Bromonaphth-2-ylthio)phenyl]-4-methoxytetrahydropyran | HCID 19764786 | 30% |
Reaction Steps
Using a similar procedure to that described in Example 12, 6-bromo-2-naphthalenethiol was reacted with 4-(3-iodophenyl)-4-methoxytetrahydropyran to give 4-[3-(6-bromonaphth-2-ylthio)phenyl]-4-methoxytetrahydropyran in 30% yield, as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05208259 |
| Source dataset | uspto-grants-1993_05 |
| ORD ID | ord-c1da82a239f242eda031b398dd9e6bb7 |
| Source note | uspto-grants-1993_05 |