HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cetyl Alcohol → Ethyl 2-[(hexadecyloxy)methyl]-2-propenoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cetyl Alcohol | HCID 2682 | — |
| Reactant | 2-Dimethylaminopyridine | HCID 21885 | — |
| Reactant | 2-(Bromomethyl)acrylic acid ethyl ester | HCID 310620 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | Ethyl 2-[(hexadecyloxy)methyl]-2-propenoate | HCID 12971817 | 261.3% |
Reaction Steps
To a stirred solution of 1.9 g of hexadecanol in 40 ml of methylene chloride containing 700 mg of dimethylaminopyridine is added 500 mg of ethyl 2-bromomethyl-2-propenoate followed by continued stirring for 18 hours. The solvent is evaporated to give 2.4 g of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05208223 |
| Source dataset | uspto-grants-1993_05 |
| ORD ID | ord-a809b9129d0249679d8a3637c3af828d |
| Source note | uspto-grants-1993_05 |