HRID248216

反应详情

EQUATION

反应方程式

HRID 248216 的结构方程式

PROCEDURE

实验过程

In the BF3 absorption tank, the isobutyryl fluoride solution absorbed BF3 contained in gas released from the acylation reactor, and no BF3 was detected in the analysis of gas purged from the BF3 absorption tank. In the complex preparation tank, the isobutyryl fluoride synthesis solution from the BF3 absorption tank further absorbed BF3 recovered from the distillation column, and in the acylation reactor, the resultant isobutyryl fluoride synthesis solution reacted with 2-methylnaphthalene to give 2-isobutyryl-6-methylnaphthalene.

WORKUP

后处理

  1. customIn the BF3 absorption tank
  2. customthe isobutyryl fluoride solution absorbed BF3
  3. custompurged from the BF3 absorption tank
  4. customIn the complex preparation tank
  5. customfrom the BF3 absorption tank further absorbed BF3
  6. distillationrecovered from the distillation column
  7. customin the acylation reactor, the resultant isobutyryl fluoride synthesis solution