HRID248216
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
PROCEDURE
实验过程
In the BF3 absorption tank, the isobutyryl fluoride solution absorbed BF3 contained in gas released from the acylation reactor, and no BF3 was detected in the analysis of gas purged from the BF3 absorption tank. In the complex preparation tank, the isobutyryl fluoride synthesis solution from the BF3 absorption tank further absorbed BF3 recovered from the distillation column, and in the acylation reactor, the resultant isobutyryl fluoride synthesis solution reacted with 2-methylnaphthalene to give 2-isobutyryl-6-methylnaphthalene.
WORKUP
后处理
- customIn the BF3 absorption tank
- customthe isobutyryl fluoride solution absorbed BF3
- custompurged from the BF3 absorption tank
- customIn the complex preparation tank
- customfrom the BF3 absorption tank further absorbed BF3
- distillationrecovered from the distillation column
- customin the acylation reactor, the resultant isobutyryl fluoride synthesis solution