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HRID248311

反应详情

EQUATION

反应方程式

HRID 248311 的结构方程式

REACTANTS

反应物

3
结构：Cc1ccccc1
HCID1140

Toluene

C7H8

结构：CCCCC[C@H]1CC[C@H](C(C)C(O)O)CC1
HCID178444477

未命名化合物

结构：O=C[C@H]1CC[C@H](C(F)(F)F)CC1
HCID178520943

未命名化合物

PRODUCTS

生成物

1
结构：CCCCC[C@H]1CC[C@H](C2COC([C@H]3CC[C@H](C(F)(F)F)CC3)OC2)CC1
HCID178444382

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O
溶剂HCID962

Water

H2O

PROCEDURE

实验过程

A mixture of 0.02 mol of tras-4-trifluoromethyl-1-formylcyclohexane (prepared as in Example 3), 0.02 mol of 2-(trans-4-pentylcyclohexyl)propanediol (prepared as in DE 3,227,916), 30 ml of toluene and 0.5 g of pTSOH is heated for 6 hours on a water separator. The product is obtained after customary work-up and crystallization.

WORKUP

后处理

  1. customThe product is obtained
  2. customafter customary work-up and crystallization