HCID 15006861, compound → HCID 15342880, compound

Participants

Reaction Steps

30 g of (7-2) thus obtained was dissolved in 600 ml of ethyl acetate. 60 g of manganese dioxide was then added to the solution. The reaction mixture was stirred at room temperature for 4 hours. The reaction mixture was filtered off at an elevated temperature, and the filtrate was then concentrated. The concentrate was recrystallized from acetonitrile to obtain 27 g of the desired compound.

Provenance & Evidence