Acetic Anhydride → HCID 178474900, compound

HRID 24854Notes

Reaction equation

HRID 24854 reaction equation
[NH2:1][CH2:2][C:3]([N:5]([C:7]1[CH:12]=[CH:11][C:10]([NH:13]/[C:14](=[C:21]2\[C:22](=[O:33])[NH:23][C:24]3[C:29]\2=[CH:28][C:27]([N+:30]([O-:32])=[O:31])=[CH:26][CH:25]=3)/[C:15]2[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=2)=[CH:9][CH:8]=1)[CH3:6])=[O:4].[C:34](OC(=O)C)(=[O:36])[CH3:35]>C(O)(=O)C>[C:34]([NH:1][CH2:2][C:3]([N:5]([C:7]1[CH:12]=[CH:11][C:10]([NH:13]/[C:14](=[C:21]2\[C:22](=[O:33])[NH:23][C:24]3[C:29]\2=[CH:28][C:27]([N+:30]([O-:32])=[O:31])=[CH:26][CH:25]=3)/[C:15]2[CH:16]=[CH:17][CH:18]=[CH:19][CH:20]=2)=[CH:9][CH:8]=1)[CH3:6])=[O:4])(=[O:36])[CH3:35]

Participants

4

Reactant 2

HCID 7918Acetic AnhydrideHCID 178485780HCID 178485780, compound

Product 1

HCID 178474900HCID 178474900, compound

Reagents, catalysts & solvents 1

HCID 176Acetic AcidSolvent

Procedure

Prepared analogously to Example 31 from (Z)-3-{1-[4-(N-aminomethylcarbonyl-N-methyl-amino)-phenylamino]-1-phenyl-methylidene}-5-nitro-2-indolinone and acetic anhydride in glacial acetic acid.

Sources & evidence

ORD record
ord-d8f655837d8e43c8bd59fdaa225bb6f6
Source dataset
uspto-grants-2005_02
Patent number
US06855710B2

Reaction notes

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