HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroquinone → 4-Hydroxyphenyl 4-allyloxybenzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroquinone | HCID 785 | — |
| Reactant | 4-Allyloxybenzoyl chloride | HCID 11790137 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 4-Hydroxyphenyl 4-allyloxybenzoate | HCID 15346429 | — |
Reaction Steps
A solution containing 78.8 g of 4-(prop-2-en-1-oxy)benzoyl chloride (obtainable according to DE-A 2,944,591) and 220.0 g of hydroquinone in 400 ml of dry tetrahydrofuran was boiled for 4 hours under reflux. After being concentrated the product was recrystallized from toluene and ethanol (1:1 parts by volume). Melting point: 146° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05211877 |
| Source dataset | uspto-grants-1993_05 |
| ORD ID | ord-2832f3787bca4e6398005a325dc6f85b |
| Source note | uspto-grants-1993_05 |