Nitric Acid → HCID 19762126, compound

Participants

Reaction Steps

11.6 g of 1,4-di(n-hexyloxy)benzene was dissolved in a mixed solvent of 50 ml of acetic anhydride and 50 ml of n-hexane, and 4 ml of concentrated nitric acid having a specific gravity of 1.42 was dropwise added thereto at a room temperature of 20° C. over 3 minutes. The internal temperature rose to 46° C., and the reaction was completed to obtain 13.1 g of 2,5-di(n-hexyloxy)nitrobenzene (yield: 97%).

Provenance & Evidence