HCID 19762580, compound → HCID 178491103, compound

Participants

Reaction Steps

Preparation is effected analogously to Example 1, using 0.54 g (1.6 mol) of N-[2-[N-(4-methoxybenzyl)-N-(2-pyridyl)amino]ethyl]-N-methyl-1,4-butanediamine and the equimolar amount of N-cyano-N'-[2-[[(2-guanidino-4-thiazolyl)methyl]thio]ethyl]-O-phenyl-isourea as starting materials. Working up by chromatography analogously to Example 1 yields the purified title compound in the form of a dry foam. MS (+FAB method): m/z (rel. int. [%])=624 ([M+H]+, 1), 121 (100) IR (KBr): 2163 cm-1 (C≡N).

Provenance & Evidence