1,1'-Carbonyldiimidazole → HCID 178483845, compound

Participants

Reaction Steps

Preparation is effected analogously to Example 63, using 0.33 g (1.05 mmol) of N-[2-[N-(4-fluorobenzyl)-N-(2-pyridyl)amino]ethyl]-N-methyl-1,3-propanediamine and the equimolar amounts of 1,1'-carbonyldiimidazole and 2-[[(2-guanidino-4-thiazolyl)methyl]thio]ethaneamine as starting materials. Working up by chromatography analogously to Example 63 yields the purified title compound in the form of a dry foam. MS (+FAB method): m/z (rel. int. [%])=574 ([M+H]+, 9), 109 (100) IR (KBr): 1682 cm-1 (C=O).

Provenance & Evidence