Acetic Acid → HCID 54218971, compound

Participants

Reaction Steps

The compound (59) (0.288 g) was dissolved in a mixed solvent (30 ml) consisting of acetic acid, water and THF (4:2:1) and the solution was kept at 45° C. for 3.5 hours. The resultant mixture was worked up with the conventional procedure and the obtained crude product was subjected to silicagel column chromatography to give the titled compound (60) Yield: 0.184 g (76%).

Provenance & Evidence