Methylhydrazine → N-(2,2,6,6-tetramethyl-4-piperidinyl)-N'-methylaminooxamide

HRID 249236Notes

Reaction equation

HRID 249236 reaction equation
[CH3:1][C:2]1([CH3:18])[CH2:7][CH:6]([NH:8][C:9](=[O:15])[C:10]([O:12]CC)=O)[CH2:5][C:4]([CH3:17])([CH3:16])[NH:3]1.[CH3:19][NH:20][NH2:21]>CO>[CH3:18][C:2]1([CH3:1])[CH2:7][CH:6]([NH:8][C:9]([C:10]([NH:21][NH:20][CH3:19])=[O:12])=[O:15])[CH2:5][C:4]([CH3:16])([CH3:17])[NH:3]1

Participants

4

Reactant 2

HCID 6061MethylhydrazineHCID 11118680ethyl N-(2,2,6,6-tetramethyl-4-piperidinyl)oxamate

Product 1

HCID 20085747N-(2,2,6,6-tetramethyl-4-piperidinyl)-N'-methylaminooxamide

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

N-(2,2,6,6-tetramethyl-4-piperidinyl)-N'-methylaminooxamide was prepared by reacting ethyl N-(2,2,6,6-tetramethyl-4-piperidinyl)oxamate with 97% methyl hydrazine in methanol.

Sources & evidence

ORD record
ord-fc057fb02e9d4d3b98f0eabaf24f283f
Source dataset
uspto-grants-1993_05
Patent number
US05213897

Reaction notes

Loading…