HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(1-benzylpiperid-4-yl)-N-methylpropionamide → N-Methyl-N-(piperidin-4-yl)propionamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(1-benzylpiperid-4-yl)-N-methylpropionamide | HCID 19761195 | — |
| Catalyst | Palladium hydroxide | HCID 9942167 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | N-Methyl-N-(piperidin-4-yl)propionamide | HCID 19761222 | 60% |
Reaction Steps
31 g of the amine obtained in Stage B are hydrogenated in 350 ml of ethanol with 1 g of palladium hydroxide at atmospheric pressure and room temperature. The mixture is filtered and evaporated to yield the desired product in the form of an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05214055 |
| Source dataset | uspto-grants-1993_05 |
| ORD ID | ord-ebdf0bba50384124b7730060a2bd1a56 |
| Source note | uspto-grants-1993_05 |