HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 19761544, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 19761518 | HCID 19761518 | — |
| Product | HCID 19761544 | HCID 19761544 | 60% |
Reaction Steps
Using the procedure described in Example 8, (2RS,3SR)-2-(5-fluoro-3-(naphth-2-ylmethoxy)phenyl]-2-methoxybutan-3-ol was reacted with methyl iodide to give (2RS,3SR)-2-(5-fluoro-3-(naphth-2-ylmethoxy)phenyl]-2-methoxybut-3-yl methyl ether in 60% yield, m.p. 75°-76° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05214069 |
| Source dataset | uspto-grants-1993_05 |
| ORD ID | ord-e775ff903d18428ab0efdbc343874b3d |
| Source note | uspto-grants-1993_05 |