HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 19088718, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | HCID 19769486 | HCID 19769486 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 19088718 | HCID 19088718 | — |
Reaction Steps
Lithium aluminium hydride (0.345 g) was added to a solution of the ester so obtained in diethyl ether (70 ml) and the mixture was stirred at ambient temperature for 1 hour. Water (10 ml) was added dropwise and the mixture was filtered. The organic layer was dried (MgSO4) and evaporated to give (-)-2-(3-benzyloxy-5-fluorophenyl)butane-1,2-diol (2.2 g), as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05214069 |
| Source dataset | uspto-grants-1993_05 |
| ORD ID | ord-c257404c875d4618a19549a18f0f98f8 |
| Source note | uspto-grants-1993_05 |