HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Carbonate → Carbonic acid, bis[2-(dimethylamino)ethyl] ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Carbonate | HCID 7766 | — |
| Reactant | 2-(Dimethylamino)ethanol | HCID 7902 | — |
| Reactant | Bis(dimethylaminoethyl) ether | HCID 18204 | — |
| Product | Carbonic acid, bis[2-(dimethylamino)ethyl] ester | HCID 76417 | — |
Reaction Steps
A process for preparing bis[2-(N,N-dimethylamino)ethyl]ether which comprises (i) contacting 2-(N,N-dimethylamino)ethanol with diethyl carbonate under conditions effective to produce bis[2-(N,N-dimethylamino)ethyl]carbonate, and (ii) contacting bis[2-(N,N-dimethylamino)ethyl]-carbonate with a magnesium:aluminum mixed metal oxide catalyst under conditions effective to produce bis[2-(N,N-dimethylamino)ethyl]ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05214142 |
| Source dataset | uspto-grants-1993_05 |
| ORD ID | ord-696a3e0ca432431dbb0c5737154e8fbe |
| Source note | uspto-grants-1993_05 |