Ethanolamine → HCID 19761793, compound

HRID 249467Notes

Reaction equation

[CH2:1]([CH2:3][NH2:4])[OH:2].[N+:5]([C:8]1[CH:16]=[C:15]([N+:17]([O-:19])=[O:18])[CH:14]=[C:13]([N+:20]([O-:22])=[O:21])[C:9]=1[C:10](Cl)=[O:11])([O-:7])=[O:6]>>[OH:2][CH2:1][CH2:3][NH:4][C:10](=[O:11])[C:9]1[C:8]([N+:5]([O-:7])=[O:6])=[CH:16][C:15]([N+:17]([O-:19])=[O:18])=[CH:14][C:13]=1[N+:20]([O-:22])=[O:21]

Participants

Reactant 2

HCID 700Ethanolamine

HCID 24126Benzoyl chloride, 2,4,6-trinitro-

Product 1

HCID 19761793HCID 19761793, compound

Procedure

In the method of preparation, one mole of ethanolamine is reacted with each mole of 2,4,6-trinitrobenzoyl chloride to produce N-(2-hydroxyethyl)-2,4,6-trinitrobenzamide which is then nitrated to form the desired N-(2-hydroxyethyl nitrate)-2,4,6-trinitrobenzamide.

Sources & evidence

ORD record: ord-ad7ce7763a0d461497c3740aeac806ad
Source dataset: uspto-grants-1993_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05214189

Reaction notes

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