関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Ethyl Lactate | HCID 7344 | — |
| 反応物 | 3,7-Dimethyl-1-octanol | HCID 7792 | — |
| 生成物 | 3,7-Dimethyl-1-octyl lactate | HCID 11535958 | 62.2% |
反応手順
A mixture of Novozym 435 (2.81 g), molecular sieves (23.17 g), 3,7-dimethyl-1-octanol (4.64 g), and ethyl lactate (14.78 g) in a 250 mL beaker was maintained at 60° C. in a convection oven for 28 hours. Upon work-up, 4.2 g of 3,7-dimethyl-1-octyl lactate (62% yield) was obtained as an amber-colored liquid. The purity of the product was >96% as assessed by HPLC-RI.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US07863025B2 |
|---|
| 出典データセット | uspto-grants-2011_01 |
|---|
| ORD ID | ord-5ef4352b11c3443e87db73d3185b8e02 |
|---|
| 出典メモ | uspto-grants-2011_01 |
|---|
