4-Methoxyphenylhydrazine hydrochloride → HCID 178492050, compound

HRID 249671Notes

Reaction equation

HRID 249671 reaction equation
[C:1]1([N:7]2[C:19](=[O:20])[C:10]3=[CH:11][NH:12][C:13]4[CH:14]=[CH:15][CH:16]=[CH:17][C:18]=4[C:9]3=[N:8]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.Cl.[CH3:22][O:23]C1C=CC(NN)=CC=1>>[CH3:22][O:23][C:4]1[CH:3]=[CH:2][C:1]([N:7]2[C:19](=[O:20])[C:10]3=[CH:11][NH:12][C:13]4[CH:14]=[CH:15][CH:16]=[CH:17][C:18]=4[C:9]3=[N:8]2)=[CH:6][CH:5]=1

Participants

3

Reactant 2

HCID 27239044-Methoxyphenylhydrazine hydrochlorideHCID 178515184HCID 178515184, compound

Product 1

HCID 178492050HCID 178492050, compound

Procedure

The title compound was prepared following the procedure described in Step 3 for the synthesis of 4a, but using 4-methoxyphenyl hydrazine hydrochloride instead of phenyl hydrazine hydrochloride. 1H NMR (DMSO-d6) δ (ppm): 3.76 (3H, s), 6.98 (1H, q, J=5.50 Hz), 7.01 (1H, d, J=9.33 Hz), 7.55 (1H, m), 7.70 (2H, m), 8.05 (1H, q, J=5.09 Hz), 8.08 (1H, d, J=9.33 Hz), 8.19 (1H, d, J=7.96 Hz), 8.70 (1H, d, J=6.31 Hz). m/z 292.4 (MH+).

Sources & evidence

ORD record
ord-71db6705be554f78b399c070075f1df1
Source dataset
uspto-grants-2011_01
Patent number
US07863266B2

Reaction notes

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