Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Trifluoroacetohydrazide → HCID 178446280, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Trifluoroacetohydrazide | HCID 229753 | — |
| 반응물 | methyl 4-(pentylamino)-1H-imidazole-5-carbimidothioate | HCID 135984704 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | HCID 178446280 | HCID 178446280 | — |
반응 단계
The mixture of methyl 4-(pentylamino)-1H-imidazole-5-carbimidothioate (0.53 g, 2.4 mmol) and trifluoroacetic acid hydrazide (0.45 g, 3.5 mmol) in ethanol (10 mL) was refluxed overnight. The reaction mixture was concentrated to yield the product as slightly green viscous oil. LCMS calculated for C11H16F3N6(M+H): 289.1. found: 289.1.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07863285B2 |
| 출처 데이터셋 | uspto-grants-2011_01 |
| ORD ID | ord-ae3d46556d5a4d618146d09e700d6d6f |
| 출처 메모 | uspto-grants-2011_01 |