HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 19689974, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | HCID 19689869 | HCID 19689869 | — |
| Product | HCID 19689974 | HCID 19689974 | 96.5% |
Reaction Steps
Using 4-amino-N-{3-[4-(4-fluorobenzoyl)piperidino]propyl}-N-(3-methoxyphenyl)benzamide (300.0 mg, 0.61 mmol) and acetic anhydride (0.069 ml, 0.73 mmol), the procedure of inventive Example 94 was repeated to obtain 312.6 mg (96.5%) of the title compound in a light yellow amorphous form.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05728835 |
| Source dataset | uspto-grants-1998_03 |
| ORD ID | ord-f0a82c402a4540cdb23dc731ebf18155 |
| Source note | uspto-grants-1998_03 |