HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 12044217, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 45095769 | HCID 45095769 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 12044217 | HCID 12044217 | 91.3% |
Reaction Steps
To a stirred solution of 10 g (0.0426 mol) of 2-bromo-1-(5-ethyl pyridin-2-yl)-ethanol dissolved in 50 mL of methanol, 6.86 g (0.0511 mol) potassium carbonate was added at 25-30° C. and stirring was continued for 1 hr. Subsequently filtered and methanol was concentrated to furnish 5.8 g (90%) of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07863300B2 |
| Source dataset | uspto-grants-2011_01 |
| ORD ID | ord-78bda8b351914b82b9a5b1093daf28ab |
| Source note | uspto-grants-2011_01 |