HuagongsheHuagongshe Chemistry Print Report · For research reference only
(Dimethyl sulfide)trihydroboron → HCID 44589528, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (Dimethyl sulfide)trihydroboron | HCID 12423031 | — |
| Reactant | HCID 12512124 | HCID 12512124 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 44589528 | HCID 44589528 | — |
Reaction Steps
In an alternate procedure, 3-(1H-Indol-3-yl)-N-methyl-3-phenyl-propionamide (0.400 g) was reduced by refluxing overnight in THF (20 ml) with excess borane-dimethylsulfide to yield [3-(1H-Indol-3-yl)-3-phenyl-propyl]-methyl-amine, which was converted to an oxalate salt (mp 123.7-134.1° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07863305B2 |
| Source dataset | uspto-grants-2011_01 |
| ORD ID | ord-c94030033f254b0c8a6fda928c53f4cf |
| Source note | uspto-grants-2011_01 |