Water → HCID 66868950, compound

Participants

Reaction Steps

Add potassium permanganate (2.49 g) to a mixture of 1-phenyl-2-(3-nitro-4-(isobutylamino)phenyl)acetylene (1.17 g), sodium bicarbonate (0.20 g), and magnesium sulfate (0.98 g), in water (5 mL) and acetone (5 mL). Stir at room temperature over night. Pour into saturated aqueous sodium sulfite, extract with ethyl acetate, dry over sodium sulfate, and concentrate under reduced pressure to provide the title compound as a red solid (0.89 g, 69%).

Provenance & Evidence