4-Amino-1-butanol → HCID 45097130, compound

HRID 251066Notes

Reaction equation

HRID 251066 reaction equation
[NH2:1][CH2:2][CH2:3][CH2:4][CH2:5][OH:6].[CH3:7][C:8]1[C:9]([CH:15]=O)=[N:10][CH:11]=[C:12]([CH3:14])[CH:13]=1.[BH4-].[Na+]>CO>[CH3:7][C:8]1[C:9]([CH2:15][NH:1][CH2:2][CH2:3][CH2:4][CH2:5][OH:6])=[N:10][CH:11]=[C:12]([CH3:14])[CH:13]=1

Participants

5

Reactant 3

HCID 258684-Amino-1-butanolHCID 4311764Sodium borohydrideHCID 187316833,5-Dimethylpyridine-2-carbaldehyde

Product 1

HCID 45097130HCID 45097130, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Using General Procedure B, 4-amino-butan-1-ol and 3,5-dimethyl-pyridine-2-carbaldehyde in MeOH were reacted with NaBH4 to give 4-[(3,5-dimethyl-pyridin-2-ylmethyl)-amino]-butan-1-ol as a pale yellow oil.

Sources & evidence

ORD record
ord-9be8cbcfafe640c1b0d05bb3eb653db8
Source dataset
uspto-grants-2011_01
Patent number
US07863293B2

Reaction notes

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