HCID 86627970, compound → HCID 67268582, compound

Participants

Reaction Steps

A solution of the amide (ZZ5) (1 eq.) in MeOH was cooled at 0° C. under N2, then Pd/C (10% wt) was added. After two vacuum-H2 cycles the mixture was stirred 2.5 hr under an H2 atmosphere. The catalyst was filtered off and washed with MeOH then the solvent was removed under reduced pressure. The crude was used as such in the following reaction. MS (ES) C20H24N4O requires: 336, found: 337 (M+H)+.

Provenance & Evidence