N-bromobutanimide → HCID 86606378, compound

Participants

Reaction Steps

Dissolving 8.5 g (19 mmol) of 4-anthracen-9-yl-6-naphthalen-1-yl-phenyl-pyrimidine obtained in the foregoing step (2) into 100 milliliter of N,N-dimethylformamide, and adding 3.6 g (20 mmol) of N-bromosuccinimide, stirred at room temperature for 8 hours. After completion of the reaction, precipitated solids were separated by filtration and washed with water and methanol, thereby obtaining 7.2 g of 4-(10-bromo-anthracen-9-yl)-6-naphthalen-1-yl-phenyl-pyrimidine (yield: 73%).

Provenance & Evidence