HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chloro-2-fluorobenzoic acid → 4-Chloro-2-fluorobenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chloro-2-fluorobenzoic acid | HCID 99152 | — |
| Reactant | 5-Chloro-2-fluorobenzamide | HCID 2773592 | — |
| Product | 4-Chloro-2-fluorobenzamide | HCID 3721849 | — |
Reaction Steps
A method similar to the preparation of 5-chloro-2-fluorobenzamide (see page 17 above) was followed using 4-chloro-2-fluorobenzoic acid (500 mg, 5.73 mmol). The title compound was isolated as an off-white solid (465 mg, 94%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07868017B2 |
| Source dataset | uspto-grants-2011_01 |
| ORD ID | ord-4b299c36ce824333845cec6832f142c4 |
| Source note | uspto-grants-2011_01 |