Sulfuryl chloride → HCID 86616719, compound
Reaction equation
[S:1]([Cl:5])(Cl)(=[O:3])=[O:2].[CH3:6][O:7][C:8]1[CH:13]=[CH:12][C:11]([C:14]2[S:15][CH:16]=[CH:17][C:18]=2[CH3:19])=[CH:10][CH:9]=1>>[CH3:6][O:7][C:8]1[CH:9]=[CH:10][C:11]([C:14]2[S:15][C:16]([S:1]([Cl:5])(=[O:3])=[O:2])=[CH:17][C:18]=2[CH3:19])=[CH:12][CH:13]=1Participants
3
Procedure
The above sulfonyl chloride, EI-MS: M=304.1, was prepared analogous to Example 50 using 2-(4-methoxy-phenyl)-3-methyl-thiophene in the first step.
Sources & evidence
- ORD record
- ord-5766e57f693c4fa9b66a39d869c0da7d
- Source dataset
- uspto-grants-2011_01
- Patent number
- US07868030B2
Reaction notes
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