3,5-Dimethoxybenzaldehyde → HCID 66842912, compound

HRID 252321Notes

Reaction equation

HRID 252321 reaction equation
C(OP([CH2:9][C:10]1[CH:15]=[C:14]([O:16][CH3:17])[C:13]([CH2:18][CH2:19][CH3:20])=[C:12]([O:21][CH3:22])[CH:11]=1)(=O)OCC)C.[CH3:23][O:24][C:25]1[CH:26]=[C:27]([CH:30]=[C:31]([O:33][CH3:34])[CH:32]=1)[CH:28]=O>>[CH3:17][O:16][C:14]1[CH:15]=[C:10]([CH:9]=[CH:28][C:27]2[CH:30]=[C:31]([O:33][CH3:34])[CH:32]=[C:25]([O:24][CH3:23])[CH:26]=2)[CH:11]=[C:12]([O:21][CH3:22])[C:13]=1[CH2:18][CH2:19][CH3:20]

Participants

3

Reactant 2

HCID 817473,5-DimethoxybenzaldehydeHCID 86036824HCID 86036824, compound

Product 1

HCID 66842912HCID 66842912, compoundYield 25%

Procedure

This material was prepared from diethyl(3,5-dimethoxy-4-1-propylbenzyl)phosphonate and 3,5-dimethoxybenzaldehyde in 25% yield as the same procedure as described in Example 5(b)

Sources & evidence

ORD record
ord-5692b47bd253401b89fd3ede4f32e1d1
Source dataset
uspto-grants-2011_01
Patent number
US07868047B2

Reaction notes

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