HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron tribromide → 5-(2-Phenylethenyl)-2-n-tetradecanyl-1,3-benzenediol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron tribromide | HCID 25134 | — |
| Reactant | 1-(3,5-Dimethoxy-4-n-tetradecanylphenyl)-2-phenylethene | HCID 66842388 | — |
| Product | 5-(2-Phenylethenyl)-2-n-tetradecanyl-1,3-benzenediol | HCID 66842936 | — |
Reaction Steps
This material was synthesized from 1-(3,5-dimethoxy-4-n-tetradecanylphenyl)-2-phenylethene and BBr3 by the same method as described in Example 6. 1HNMR (CDCl3, ppm): δ0.95 (m, 6H), 1.30 (m, 22H), 2.65 (m, 2H), 4.80 (s, 2H), 6.60 (s, 2H), 7.00 (s, 2H), 7.26 (m, 1H), 7.36 (m, 2H), 7.52 (m, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07868047B2 |
| Source dataset | uspto-grants-2011_01 |
| ORD ID | ord-999fb6cb292642dd88bd029bc2137960 |
| Source note | uspto-grants-2011_01 |