HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromo-2,6-difluorobenzene → 1-(2,6-Difluorophenyl)-2-(3,5-dimethoxy-4-1-propylphenyl)ethene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromo-2,6-difluorobenzene | HCID 123557 | — |
| Reactant | (3,5-Dimethoxy-4-1-propylphenyl)ethene | HCID 66842614 | — |
| Product | 1-(2,6-Difluorophenyl)-2-(3,5-dimethoxy-4-1-propylphenyl)ethene | HCID 66842656 | — |
Reaction Steps
This compound was synthesized from (3,5-dimethoxy-4-1-propylphenyl)-ethene and 1-bromo-2,6-difluorobenzene quantitatively in the same procedure as described in preparation of 31B. 1HNMR (CDCl3, ppm): δ 1.32 (d, J=7.1 Hz, 6H), 3.62 (qint, J=7.1 Hz, 1H), 3.90 (s, 6H), 6.73 (s, 2H), 6.8-7.2 (m, 4H), 7.41 (d, J=16.6 Hz, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07868047B2 |
| Source dataset | uspto-grants-2011_01 |
| ORD ID | ord-4bafab4dd0c84a1c8edc9c8188032892 |
| Source note | uspto-grants-2011_01 |