HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methoxypropyne → HCID 66889153, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methoxypropyne | HCID 69393 | — |
| Reactant | HCID 11772326 | HCID 11772326 | — |
| Product | HCID 66889153 | HCID 66889153 | — |
Reaction Steps
Analogously to residue 9a, 9.31 g of 5-bromobenzofuran-3-yl trifluoromethanesulphonate [440083-74-9] and 3.52 ml of 3-methoxypropyne are reacted. The title compound is obtained as a yellowish oil. Rf=0.43 (1:10 EtOAc-heptane). Rt=5.14 (gradient I).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07868036B2 |
| Source dataset | uspto-grants-2011_01 |
| ORD ID | ord-7385b0b718854e4ea3b4c81ecaa2043d |
| Source note | uspto-grants-2011_01 |