HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Aminobenzoic Acid → 4-(dodecanoylamino)benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Aminobenzoic Acid | HCID 978 | — |
| Reactant | Dodecanoyl chloride | HCID 8166 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | 4-(dodecanoylamino)benzoic acid | HCID 4694979 | 89.6% |
Reaction Steps
4-Aminobenzoic acid (0.94 g, 6.85 mmol) was dissolved in 5 mL of pyridine and dodecanoyl chloride (1.58 mL, 6.85 mmol) was added. The mixture was stirred for 4 h at room temperature. The product was precipitated by dilution with water (50 mL), filtered, and dried to provide 1.96 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07868135B2 |
| Source dataset | uspto-grants-2011_01 |
| ORD ID | ord-d68f8935c0bc4d519eba087c9a86eeb3 |
| Source note | uspto-grants-2011_01 |