HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methoxybenzenesulfonyl chloride → HCID 86620409, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methoxybenzenesulfonyl chloride | HCID 7401 | — |
| Reactant | HCID 86244444 | HCID 86244444 | — |
| Product | HCID 86620409 | HCID 86620409 | — |
Reaction Steps
Using an analogous procedure to that described in Example 83, N-[5-(5-aminopyridin-2-yl)-4-methyl-1,3-thiazol-2-yl]acetamide was reacted with 4-methoxyphenylsulfonyl chloride to give the title compound; 1H NMR Spectrum: (DMSOd6) 2.13 (s, 3H), 2.47 (s, 3H), 3.81 (s, 3H), 7.09 (d, 2H), 7.55 (m, 2H), 7.73 (d, 2H), 8.26 (m, 1H), 10.42 (s, 1H), 12.05 (s, 1H); Mass Spectrum: M+H+ 419.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07868188B2 |
| Source dataset | uspto-grants-2011_01 |
| ORD ID | ord-9a02446a1fba4babba6ddd72617e7ea0 |
| Source note | uspto-grants-2011_01 |