1-Methylpiperazine → HCID 178480641, compound

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Reaction Steps

The title compound was prepared following the procedure described for 7a using 1-methylpiperazine instead of piperazine. 1H-NMR (DMSO-d6) δ (ppm): 3.25 (4H, br), 3.41 (3H, s), 3.52 (4H, br), 7.12 (1H, t, J=7.47 Hz), 7.39 (3H, m), 7.45 (1H, m), 7.68 (1H, m), 8.22 (2H, dd, J=8.55, 0.98 Hz), 8.60 (1H, d, J=5.86 Hz), 9.12 (1H, br). m/z 346.4 (MH+). m/z 360.4 (MH+).

Provenance & Evidence