HCID 178507347, compound → HCID 178507348, compound

HRID 252947Notes

Reaction equation

HRID 252947 reaction equation
NC1C=CC2NC=C3C(=O)N(C4C=CC=CC=4)N=C3C=2C=1.[Cl:22][C:23]1[CH:28]=[CH:27][C:26]([N:29]2[C:44](=[O:45])[C:32]3=[CH:33][NH:34][C:35]4[CH:36]=[CH:37][C:38]([N+:41]([O-])=O)=[CH:39][C:40]=4[C:31]3=[N:30]2)=[CH:25][CH:24]=1>>[NH2:41][C:38]1[CH:37]=[CH:36][C:35]2[NH:34][CH:33]=[C:32]3[C:44](=[O:45])[N:29]([C:26]4[CH:25]=[CH:24][C:23]([Cl:22])=[CH:28][CH:27]=4)[N:30]=[C:31]3[C:40]=2[CH:39]=1

Participants

3

Reactant 2

HCID 178507347HCID 178507347, compoundHCID 178515217HCID 178515217, compound

Product 1

HCID 178507348HCID 178507348, compound

Procedure

The title compound was prepared following the procedure described for 6a using 5b. 1H-NMR (DMSO-d6) δ (ppm): 7.19 (1H, tt, J=7.32, 1.22 Hz), 7.44 (4H, m), 8.22 (4H, m), 8.48 (1H, d, J=6.59 Hz). m/z 311.8 (MH+).

Sources & evidence

ORD record
ord-78a0f67e80834abfbafb49cb110e2d24
Source dataset
uspto-grants-2011_01
Patent number
US07872002B2

Reaction notes

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