HCID 178507230, compound → HCID 178515225, compound

HRID 252956Notes

Reaction equation

HRID 252956 reaction equation
[C:1]1([N:7]2[C:25](=[O:26])[C:10]3=[CH:11][NH:12][C:13]4[CH:14]=[C:15]([N:19]5[CH2:24][CH2:23][NH:22][CH2:21][CH2:20]5)[CH:16]=[CH:17][C:18]=4[C:9]3=[N:8]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.NC1C=CC2C3C(C(=O)N(C4C=CC([Cl:47])=CC=4)N=3)=CNC=2C=1>>[Cl:47][C:4]1[CH:5]=[CH:6][C:1]([N:7]2[C:25](=[O:26])[C:10]3=[CH:11][NH:12][C:13]4[CH:14]=[C:15]([N:19]5[CH2:20][CH2:21][NH:22][CH2:23][CH2:24]5)[CH:16]=[CH:17][C:18]=4[C:9]3=[N:8]2)=[CH:2][CH:3]=1

Participants

3

Reactant 2

HCID 178507230HCID 178507230, compoundHCID 178515224HCID 178515224, compound

Product 1

HCID 178515225HCID 178515225, compound

Procedure

The title compound was prepared following the procedure for 14a using 13b. 1H-NMR (DMSO-d6) δ (ppm): 3.07 (2H, br), 3.38 (4H, br), 3.48 (2H, br), 7.12 (1H, br), 7.48 (3H, m), 8.07 (1H, d, J=9.06 Hz), 8.25 (2H, dd, J=9.07, 2.20 Hz), 8.62 (1H, d, J=6.32 Hz). m/z 380.9 (MH+).

Sources & evidence

ORD record
ord-cb37bf33815a413b9a155e3df714cedc
Source dataset
uspto-grants-2011_01
Patent number
US07872002B2

Reaction notes

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