(4-Methoxyphenyl)hydrazine → HCID 178492055, compound

HRID 252963Notes

Reaction equation

HRID 252963 reaction equation
[F:1][C:2]1[CH:11]=[CH:10][C:9]2[NH:8][CH:7]=[C:6]3[C:12](=[O:21])[N:13]([C:15]4[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=4)[N:14]=[C:5]3[C:4]=2[CH:3]=1.[CH3:22][O:23]C1C=CC(NN)=CC=1>>[F:1][C:2]1[CH:11]=[CH:10][C:9]2[NH:8][CH:7]=[C:6]3[C:12](=[O:21])[N:13]([C:15]4[CH:20]=[CH:19][C:18]([O:23][CH3:22])=[CH:17][CH:16]=4)[N:14]=[C:5]3[C:4]=2[CH:3]=1

Participants

3

Reactant 2

HCID 77023(4-Methoxyphenyl)hydrazineHCID 178515196HCID 178515196, compound

Product 1

HCID 178492055HCID 178492055, compound

Procedure

The title compound was prepared following procedure for 23a using 4-methoxy phenylhydrazine instead of phenyl hydrazine. 1H-NMR (DMSO-d6) δ (ppm): 7.05 (3H, m), 7.52 (1H, dt, J=8.52, 3.02 Hz), 7.80 (1H, dd, J=9.07, 4.94 Hz), 7.88 (1H, dd, J=9.06, 2.75 Hz), 8.05 (2H, m), 8.74 (1H, d, J=5.49 Hz). m/z 310.3 (MH+).

Sources & evidence

ORD record
ord-715d83f455984133a99766426a96480f
Source dataset
uspto-grants-2011_01
Patent number
US07872002B2

Reaction notes

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