HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Dimethylpiperidine → HCID 178425481, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Dimethylpiperidine | HCID 118259 | — |
| Reactant | HCID 178515218 | HCID 178515218 | — |
| Reactant | HCID 178515226 | HCID 178515226 | — |
| Product | HCID 178425481 | HCID 178425481 | — |
Reaction Steps
The title compound was prepared following the procedure described in the synthesis of 28a using 27a and 3,5-dimethylpiperidine. 1H-NMR (DMSO-d6) δ (ppm): 0.99 (6H, d, J=6.33 Hz), 1.80 (4H, br), 2.47 (2H, t, J=8.62 Hz), 3.46 (2H, brd, J=11.81 Hz), 7.13 (1H, m), 7.26 (1H, d, J=7.97 Hz), 7.40 (2H, t, J=7.69 Hz), 7.79 (1H, d, J=13.18 Hz), 8.19 (2H, d, J=7.69 Hz), 8.65 (1H, s). m/z 391.5 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07872002B2 |
| Source dataset | uspto-grants-2011_01 |
| ORD ID | ord-8d41404c7e3d4b46be7229b73018ea14 |
| Source note | uspto-grants-2011_01 |