Hexahydro-1,4-diazepine → HCID 178515222, compound

Participants

Reaction Steps

The title compound was prepared following the procedure described in the synthesis of 28a using 27a and homopiperazine. 1H-NMR (DMSO-d6) δ (ppm): 1.98 (2H, brm), 2.48 (2H, brm), 2.67 (2H, brm), 3.45 (4H, brm), 7.15 (2H, m), 7.40 (2H, m), 7.76 (1H, d, J=2.91 Hz), 8.20 (2H, m), 8.64 (1H, s). m/z 378.2 (MH+).

Provenance & Evidence