HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-((Tert-butoxy)carbonyl)pyrrolidine-3-carboxylic acid → HCID 178441299, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-((Tert-butoxy)carbonyl)pyrrolidine-3-carboxylic acid | HCID 2760529 | — |
| Reactant | 2-tert-Butyl-4-butylisothiazol-5(2H)-imine | HCID 66867228 | — |
| Product | HCID 178441299 | HCID 178441299 | — |
Reaction Steps
The product from Example 92B and 1-(tert-butoxycarbonyl)pyrrolidine-3-carboxylic acid (Aldrich) were processed using the method described in Example 92C to afford the title compound. 1H NMR (DMSO-d6) δ 0.91 (t, J=7.3 Hz, 3H), 1.27-1.35 (m, 2H), 1.39 (s, 9H), 1.55-1.65 (m, 12H), 2.06-2.11 (m, 2H), 2.62-2.67 (m, 2H), 3.19-3.30 (m, 2H), 3.45-3.54 (m, 2H), 8.56 (s, 1H). MS (ESI+) m/z 410 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07872033B2 |
| Source dataset | uspto-grants-2011_01 |
| ORD ID | ord-42f136e174bb4523ac93a98b9dfcde29 |
| Source note | uspto-grants-2011_01 |