(+-)-alpha-Methyltryptamine → HCID 23113507, Verbindung

HRID 253732Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 253732
[NH:1]1[C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[C:3]([CH2:10][CH:11]([NH2:13])[CH3:12])=[CH:2]1.[F:14][C:15]1[CH:16]=[C:17]([CH:20]=[CH:21][CH:22]=1)[CH:18]=O>>[F:14][C:15]1[CH:16]=[C:17]([CH:18]2[C:2]3[NH:1][C:9]4[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=4)[C:3]=3[CH2:10][CH:11]([CH3:12])[NH:13]2)[CH:20]=[CH:21][CH:22]=1

Komponenten

3

Versuchsvorschrift

In addition, the compounds in Example 15(5) and Example 15(6) were prepared by separating diastereomer mixture which was obtained by reacting [2-(1H-indol-3-yl)-1-methylethyl]amine with 3-fluorobenzaldehyde, by column chromatography on silica gel.

Aufarbeitung

  1. customIn addition, the compounds in Example 15(5) and Example 15(6) were prepared
  2. customby separating diastereomer mixture which
  3. customwas obtained

Quellen und Nachweise

ORD-Eintrag
ord-60dec57d4e8548f48b41f1b46c358d0c
Quelldatensatz
uspto-grants-2011_01
Patentnummer
US07872133B2

Notizen zur Reaktion

Wird geladen…